Batch Distillation


Introduction


After completing the intial exploration of the LEGO Dacta kit, the capabilities and limitations of future projects were found. Being a Chemical Engineer, it was difficult to find any engineering aspects of the LEGOs that could be applied to this discipline. The LEGOs seemed to fit in better with the mechanical and electrical engineering backgrounds of my lab partners. However, given the limitations of the LEGOs in the field of Chemisty, it is still possible to design some interesting projects. One such project is a mini-scale batch distillation drum. This project would fit well within the limits of the LEGO kits, while giving a freshman engineer an introduction to basic chemical engineering.

Project Description


Using the LEGO kit, a very simple batch distillation drum can be built. The actual construction of the model will involve mechanical engineering. Motors and pulleys will have to be arranged in order to open and close valves on the drum in order to release the vapor and liquid contents after distillation has been completed. The theory behind the project will involve chemical engineering. As it is only a model, water will be used as the feed. A container within an insulated, LEGO shell will act as the distillation chamber. This chamber should be completely sealed during operation. It should have to closable outstreams, one for the vapor component and one for the liquid component. Also, there should be a means of refilling the chamber after a distillation is completed. A temperature sensor is placed within the chamber, along with a heat source that can heat the drum.
The actual operation of the apparatus should be fully automated through use of a computer program. After an initial charge of fluid is injected into the chamber, the heat source is turned on. The temperature is monitored until an equilibrium value is reached. Ideally, if two components were being separated, such a value would be reached, but in this case, a temperature should be set. Once this temperature is reached, the two valves are opened, with both streams being collected in separate containers. The chamber is flushed of its contents, a new batch is installed, and the process repeated.
This project emphasizes the theory behind the design of the project. Basic mass balances will have to be solved in order to size the containers used. Energy considerations will have to be addressed in order that the LEGOs are not melted by the heat source. Also, a freshman would learn the basic concept of distillation while designing the project.
Besides just distillation, if the appropriate equipment could be obtained, this project could be expanded to a batch reactor. Using the much alluded to pH meter, a simple acid-base reaction could take place within the reactor and the pH monitored instead of the temperature. A heat source may again be used to start the reaction, but the vapor exit would be eliminated.

Conclusion


Given the limitations of the LEGO Dacta kits, only simple chemical engineering designs are possible. It is very unlikely a freshman engineer would be able to design an entire distillation column or manufacturing process. A batch distillation or reactor is simple enough that it can be modeled on a small scale. While teaching the basics of engineering design, it would also introduce the concepts of chemical engineering. There would not be much of a possibility for a competition in this project, unless the projects were evaluated on efficiency and economic considerations.


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